Journal of Dental Medicine

---

The formation of oxides on the surface of the metal are proven to contribute to the formation of strong bonding. However, The base metal alloys are expected to exhibit more oxidation than high gold alloys, increase in oxide layer thickness due to repeated firing in them can reduce the bond strength. The aim of this study was to compare the effect of repeated porcelain firing on the bond strength of two base metal alloys (Minalux and Verabond II). Sixteen metal plates (20x5x0.5) from each alloy were cast and prepared according to the manufacturers' instruction. Porcelain with uniform thickness (Imm) was applied on the middle one third of metal plates. After this stage, each alloy group divided to three subgroups. Group I was fired for the second time to form the final glaze, group II and III were fired two and four more times respectively. Specimens were subjected to 3-point flexural test in a digital tritest machine. Results showed no significant differences between bond strength of two alloys. Also results showed repeated firing had no significant effect on bond strength. Due to these findings, this study support similarity of two alloys (Minalux and Verabond II) in their bond strength with porcelain.

---

Due to the differences in the composite and morphology of dentin in primary and permanent teeth, it is necessary to make improvements in bonding techniques to promote the strength of composite resins bonded to the dentinal surface, in primary teeth. The use of lower radiation, to make structural and chemical changes in dentinal surfaces has been investigated. This research was conducted to evaluate the shear strength of the composite bonded to primary teeth dentin after Nd: YAG laser radiation and acid etching for conditioning. Peripheral dentin of the buccal and lingua! surfaces of 60 extracted posterior primary teeth were exposed and polished with 600 grit with Sic paper. The teeth were divided randomly in 3 groups of 20 teeth. In group 1 etching gel, primer and adhesive of scotch bond multipurpose system (SMP), in group 2 laser at 1.6 w and 80 mj/pulse, and in group 3 laser at 2 s and 700 mj/pulse were used. Moreover, in groups 2 and 3, after laser radiation, acid etching, primer and adhesive of SMP system were applied. After necessary laboratory tests, the mean shear bond strength in MPa were 20.99±5.3 (group 1), 23.82±6.31 (group 2) and 26.58±5.59 (group 3). ANOVA, scheffe, tukey statistical tests showed that the bond strengths of group 3 were statistically higher than group 1. The frequency of dentin cohesive failures were significantly higher in groups 2 and 3, compared to group 1 that indicates a higher bond strength in these groups. Scanning electron mirographs of laser radiated surfaces, show a porous and rough surface morphology that enhances the mechanical bond of the composite.

---

Composite resin restorative materials, that nowadays are used as tooth-colour materials, have both benefits and weaknesses. One of these weaknesses is the contraction resulted from resin polymerization which influences on the composite dentin bond strength and it has been tried to be eliminated by different bonding systems. The aim of this in-vitro study was to compare the dentin bond strength of two dentine adhesive systems: multi-step Scoth Bond Multipurpose (SBMP) and single- step Excite, by two composites of Ideal Makoo and Tetric. One hundred sixty (160) sound human molars were selected. At first they were debrided and mounted with acrylic resin in molds. The enamel of the buccal surface was eliminated by diamond burs. To provide a flat dentin surface, it was removed about lmm. Then, based on the type of dentin adhesive, they were divided into two groups of 30 teeth and were applied on the exposed dentine surface according to the manufacturer's instructions. Then, each group was divided into two subgroups of 15, based on the type of composite resin. Cylinders of the desired composite resin, attached to the dentin surface, were used for 80 seconds. The samples were stored in 100% humidity (37°c) for 24 hours. The bond strengths was measured by a cross head blade with the speed of 2mm/min. Variance analysis and Duncan test, with 95% confidence level, showed that statistically, two factors of adhesive and composite, interact on each other, in bond strength. There was no significant difference in bond strength, between two composites with similar adhesives, however, comparing two different adhesives with the same composite, showed that the bond strength of Tetric with Excite (28.39) was more than that of SBMP (17.98 Mpa). Finally, it was recognized that among four experimental groups, there was only a significant difference in bond strengths, between Tetric-Excite with Tetric- SBMP. This study shows that dentin bond strength is influenced by dentin bonding agents, composite type and dentin structure, and using a type of composite with a dentin bonding agent, manufactured by the same company, results in a higher bond strength.

---

Recently. Minalux alloy, a base metal free from Be, has been presented on the market while no special soldering has been recommended for it. On the other hand, based on the manufacturer's claim, this alloy is similar to Verabond2. The aim of this study was to investigate the tensile strength of Minalux and Verabond2, soldered by Verasolder. Twelve standard dambble shape samples, with the length of 18 mm and the diameter of 3mm, were prepared from each alloy. Six samples of each alloy were divided into two pieces with carboradom disk. Soldering gap distance was 0.3mm, measured by a special jig and they were soldered by Verasolder alloy. Six other samples, of both Iranian and foreign unsoldered alloys were considered as control group. Then samples were examined under tensile force and their tensile strength was recorded. Two- way variance analysis showed that the tensile strength of Minalux alloy and Verabond2 were not statistically significant (Verasoler 686, Minalux 723), but after soldering, such difference became significant (Minalux 308, Verabond2 432). Verabond2 showed higher tensile strength after soldering.

---

Statement of Problem: Porcelain restorations are susceptible to fracture and a common method for repairing is the use of silane and composite on etched porcelain. Although HF is very effective in porcelain etching but has detrimental effects on tissues.

Purpose: In this study, the effect of APF and PHA was compared with HF in porcelain etching. Also the role of silane, unfilled resin and dentin bonding in bond strength of composite- porcelain was evaluated.

Methods and Materials: In this experimental in-vitro study, one-hundred twenty porcelain square blocks (552 mm) were prepared and bonding surfaces of each sandblasted. Samples were divided into three groups. The first group (n=40) were etched with buffered HF 9.5% (Ultradent) for 1 min., the second group (n=40) were etched with Iranian APF 1.23% (Kimia) for 10 minutes and the third group (n=40) were etched with Iranian PHA 37% (Kimia) for 1 min. Ultradent silane was applied on the surfaces of half of cases in each group. On the surfaces of half of silane-treated samples unfilled resin was applied and dentin bonding was used on the surfaces of the remaining. Samples without silane were treated in a similar manner. Composite cylinder with 4mm diameter and 2 mm height was bonded to porcelain. Specimens were stored in 37°C distilled water for 24 hours and subjected to 500 cycles. Shear bond strength was measured with an Instron machine and type of fracture was evaluated using a stereomicroscope. Results were analyzed using 3 way ANOVA, Kaplan- Maier and Tukey HSD tests.

Results: Findings showed that PHA and APF roughened the porcelain surface without creating retentive micro undercuts but HF etches porcelain and creates retentive microundercuts. Ultradent silane had no significant effect on bond strength of porcelain- composite. Unfilled resin with Ultradent silane compared with dentin bonding with the same silane is more effective in bond strength of composite- porcelain.

Conclusion: Based on present study, application of Ultradent silane on sandblasted and etched porcelain with PHA or APF cannot be used as an alternative to this silane on sandblasted and etched porcelain with HF.

---

Statement of Problem: One of the greatest problems in metal –ceramic restorations is debonding of porcelain from dental alloys. Production of dental alloys by Iranian companies necessitates the evaluation of physical and handling properties of these products.

Purpose: In this study the bond strength between porcelain and two types of base metal alloys, Supercast (with beryllium) and Minalux (without beryllium) was investigated.

Materials and Methods: In this experimental study 10 cylindric bars from each base metal alloy were prepared. The bars were degassed and porcelain was applied around them in a disc form (8 mm diameter and 2 mm thickness). The bond strength of porcelain to metal bars was tested with the shear strength test by Instron. Data were analyzed with student t-test and P<0.05 was considered as the limit of significance.

Results: The mean failure load was 71.58±6.4 KgF for Supercast and 67.34±5.48 for Minalux alloy. The bond strength of Supercast and Minalux were 55.85±4.99 MPa and 52.54±4.27 MPa respectively. The difference was statistically significant (P0.001).

Conclusions: This study showed that nickel-chromium-beryllium alloy (Supercast) produced significantly better ceramometal bonding than nickel chromium alloy without beryllium (Minalux).

---

Statement of Problem: Blood contamination is a common problem in dentistry that can decrease bond strength dramatically which may be affected by methods of decontamination as well.

Purpose: The aim of this study was to evaluate and compare the influence of blood contamination on shear bond strength of composite and compomer to dentin using Prompt L-Pop as an adhesive system. Also, to assess the effectiveness of different surface treatments on the bond strength.

Materials and Methods: In this experimental study, 120 molar teeth were sectioned to provide flat occlusal dentinal surfaces. Specimens were embedded in acrylic resin with the flat surface exposed. The dentinal expose surfaces were polished to 600 grit. The teeth were randomly divided into five groups of twelve specimens (F1–F5) for compomer material and five other groups (Z1- Z5) for composite resin. After application of Promt L-Pop to dentinal surfaces of specimens, the surfaces in all groups, except for F1 and Z1, (as controls) were contaminated with human blood and then one of the following surface treatments was applied. Groups F2 and Z2 without any treatment, groups F3 and Z3 rinsing with water, groups F4 and Z4 rinsing with water and reapplication of adhesive, groups F5 and Z5 rinsing with NaOCl and using Prompt L-Pop again. Restorative materials were applied to treated surfaces using plastic molds. After thermocycling, shear bond strengths, mode of failures and morphology of dentin-material interfaces were evaluated. The data were statistically analyzed using Factorial analysis of Variance, One-Way ANOVA, Duncan, T-student and Chi-Square tests with P<0.05 as the limit of significance.

Results: Compomer showed statistically significant higher bond strength in comparison to composite (P<0.001). Duncan test showed significant differences between all compomer groups, except between groups F4 and F5, and between all composite groups except for groups Z1 and Z4 and for groups Z2 and Z3.

Conclusion: Based on the findings of this study, shear bond strength of compomer material was significantly higher than composite. Blood contamination reduced bond strength, but rinsing contaminated dentin with water or NaOCl and reusing Prompt L-Pop increased bond strength in both materials.

---

Statement of Problem: Ceramic restorations are popular because they can provide the most natural replacement for teeth. However, the brittleness of ceramics is a primary disadvantage. There are various methods for strengthening ceramics such as metal framework, ceramic cores, and surface strengthening mechanisms through glazing, work hardening and ion exchange.

Purpose: The purpose of this study was to evaluate the effect of polish on flexural strength of feldspathic porcelain and to compare it with overglaze and autoglaze.

Materials and Methods: In this experimental study, one brand of feldspathic porcelain (colorlogic, Ceramco) was used and forty bars (25×6×3 mm) were prepared according to ISO 6872 and ADA No. 69. The specimens were randomly divided into four groups: overglazed, auto glazed, fine polish and coarse polish (clinic polish). Flexural strength of each specimen was determined by three point bending test (Universal Testing Machine, Zwick 1494, Germany). Collected data was analyzed by ANOVA and post-hoc test with P<0.05 as the limit of significance.

Results: A significant difference was observed among the studied groups (P<0.0001). According to post-hoc test, flexural strength in overglaze and fine polish group were significantly stronger than clinic polish and autoglaze group (P<0.001). Although the mean value for overglazed group was higher than fine polish group, this was not statistically significant (P=0.9). Also no statistical difference was seen between autoglazed and coarse polish group (P=0.2).

Conclusion: Based on the findings of this study, flexural strength achieved by fine polish (used in this study) can compete with overglazing the feldespathic porcelains. It also can be concluded that a final finishing procedure that involves fine polishing may be preferred to simple staining followed by self-glazing.

---

Background and Aim: Cementation is one of the most critical steps of the porcelain restoration technique. However, limited information is available concerning the bond strength of current ceramic bonding systems. The aim of this study was to evaluate the shear bond strength of three dual-cure resin cements to IPS-Empress2 ceramics.

Materials and Methods: In this experimental study, 30 pairs of IPS-Empress 2 ceramic discs were fabricated with 10 and 8 mm diameters and 2.5 mm thickness. After sandblasting and ultrasonic cleaning, the surfaces of all specimens were etched with 9% hydrofluoric acid for 60 seconds. Then, the three groups of 10 bonded specimens were prepared ceramic bonding resin systems including Panavia F2, Variolink II and Rely X ARC. After storage in 37±1c water for 24 hours and thermocycling in 5c and 55c water for 500 cycles with 1-minute dwell time, the shear bond strengths were determined using Instron machine at speed of 0.5mm/min. Data were analyzed by One Way ANOVA test. For multiple paired comparisons, the Tukey HSD method was used. The mode of failure was evaluated by scanning electro microscope (SEM). P<0.05 was considered as the limit of significance.

Result: Significant differences were found between different cement types (P<0.05). Variolink II provided the highest bonding values with IPS-Empress2. A combination of different modes of failure was observed.

Conclusion: Based on the results of this study, according to the highest mode of cohesive failure, Variolink II seems to have the strongest bond with IPS-Empress2 ceramics.

---

Background and Aim: The improvement of the physical and chemical properties of resins as well as great advances achieved in the field of chemical bonding of resin to metal has changed the trend of restorative treatments. Today the second generation of laboratory resins have an important role in the restoration of teeth. The clinical bond strength should be reliable in order to gain successful results. In this study the shear bond strength (SBS) between targis (a ceromer) and two alloys (noble and base metal) was studied and the effect of thermocycling on the bond investigated.

Materials and Methods: In this experimental study, alloys samples were prepared according to the manufacturer. After sandblasting of bonding surfaces with 50µ AI2o3 Targis was bonded to the alloy using Targis I link. All of the samples were placed in 37°C water for a period of 24 hours. Then half of the samples were subjected to 1000 cycles of thermocycling at temperatures of 5°C and 55°C. Planear shear test was used to test the bond strength in the Instron machine with the speed rate of 0.5mm/min. Data were analyzed by SPSS software. Two-way analysis of variance was used to compare the bond strength among the groups. T test was used to compare the alloys. The influence of thermocycling and alloy type on bond strength was studied using Mann Whitney test. P<0.05 was considered as the limit of significance.

Result: The studied alloys did not differ significantly, when the samples were not thermocycled (P=0.136) but after thermocycling a significant difference was observed in SBS of resin to different alloys (P=000.1). Thermal stress and alloy type had significant interaction, with regard to shear bond strength (P=0.003). There was a significant difference in SBS before and after thermocycling in noble alloys (P=0.009), but this was not true in base metals (P=0.29). Maximum SBS (19.09 Mpa) belonged to Degubond 4, before thermocycling. Minimum SBS (8.21 Mpa) was seen in Degubond 4 after thermocycling.

Conclusion: The effect of thermocycling in reducing bond strength of resin to metal depends on the type of alloy. The noble metal studied is significantly affected by thermal tensions.

---

Background and Aim: Iranian temporary cement, Tem Band, has been manufactured by Golchai company, and introduced to market as a suitable material but its properties have not been tested yet. The aim of this study was to investigate the setting time, film thickness, compressive strength, disintegration and arsenic content of Tem Band and Temp bond temporary cements and compare them to ISO 3107. Materials and Methods: In this experimental study, 12 samples from each cement were obtained and setting time, film thickness, compressive strength, solubility and disintegration were tested according to ISO 3107. In addition, arsenic content was tested based on ASTM 6052. Data were analyzed with t-test and p<0.05 was considered as the limit of significance.

Results: The average setting time of Tem Band was 5 minutes and 47 seconds (4.17 minutes for Temp Bond), the average film thickness was 6.67 micrometer for Tem Band and 4.08 micrometer for Temp Bond. There was no difference between two cements regarding setting time and film thickness and for both was at the standard range. Compressive strength of Tem Band was 5.67 MPa and 8.5 MPa for Temp Bond. The difference was statistically significant but for both cements was less than standard (35 MPa). There was no significant difference regarding the solubility and disintegration tests. In both samples, the solubility and disintegration values were in standard ranges. Both cements did not contain arsenic but lead level was at the maximum standard range in Tem Band.

Conclusion: Considering these results, both cements are applicable to different clinical situations based on their physical properties. Studies on the biocompatibility of the Iranian cement is recommended.

---

Background and Aim: Use of provisional restorations is one of the important phases in the treatment of patients who need fixed prosthesis. Some physical properties are required for these materials. The purpose of this study was the comparison of some physical properties of 4 kinds of resins: Trim, Tempron, Duralay (Aria Dent) and Acropars TRII.

Materials and Methods: In this experimental study, transverse-strength (TS), setting time (ST), polymerization shrinkage (PS) and temperature rise (TR) during polymerization were tested. In transverse strength test, 5 samples of each resin were made. TS testing was done with an Instron testing machine. ST testing (5 samples in each group) was done with Gilmore needle. In PS test, 11 cylindric samples were prepared from each resin and the shrinkage was examined with digital micrometer (up to 24 hours). In TR test, after mixing the powder and liquid of resins (8 samples in each group), the temperature rise was recorded with 10 seconds interval (up to 15 minutes). Data were analyzed with one-way ANOVA and Tukey HSD tests with p<0.05 as the limit of significance.

Results: In TS test, all samples of Trim were bent and no fracture was observed, while Tempron and Duralay showed no significant difference. Both Tempron and Duralay revealed high significant difference with Acropars TRII (P <0.01). In ST test, the difference between groups was significant (P<0.01). The lowest ST was observed in Acropars TRII (7 min), and the highest in Tempron (9.53 min). In PS test, significant difference was observed between Trim and Acropars TRII (P<0.01). PS was completed after 120 min in Tempron and Trim groups. However, PS continued to increase in other groups. In TR test, the difference between groups was significant (P<0.05). Duralay showed the highest TR and the lowest was seen in Trim.

Conclusion: In this study, Trim showed better properties than other studied groups. Acropars TRII had the lowest strength. The highest temperature rise was recorded for Duralay and Tempron, respectively.

---

Background and Aim: All ceramic, inlay-retained resin bonded fixed partial denture is a conservative method for replacement of missing teeth, because of minimal tooth reduction. The connector between the retainer and the pontic is the weak point of these bridges. Reinforcement of ceramic core will increase the clinical longevity. The aim of this study was to determine the effect of zirconia on flexural strength of IPS Empress 2 core ceramic.

Materials and Methods: In this experimental in vitro study, twenty eight bar shape specimens (17´3.1´3.1 mm) were made of four different materials: (1) Slip casting in-ceram alumina core (control group) (2) Hot-pressed lithium disilicate core ceramic (IPS Empress 2) (3) IPS Empress 2 with cosmopost (zirconia post) inserted longitudinally in the center of the bar (4) IPS Empress 2 with cosmopost (zirconia post) inserted longitudinally in bottom of the bar. Specimens were subjected to three-point flexure loading with the span of 15mm, at a cross-head speed of 0.5 mm/min. Failure loads were recorded and analyzed using one-way ANOVA and Tomhane Post-hoc tests and p<0.05 was set as the level of significance. Fractured surfaces were then observed by scanning electron microscope (SEM). Four additional samples were made as the third group, and zirconia-IPS interface was observed by SEM before fracture.

Results: Mean values and standard deviations of three point flexural strengths of groups 1 to 4, were: 378.4±44.6, 258.6±27.5, 144.3±51.7, 230±22.3 MPa respectively. All the groups were statistically different from each other (P<0.05), except groups 2 and 4. The flexural strengths of groups 2, 3, 4 were significantly lower than group 1. Group 3 had the lowest flexural strength. SEM analysis showed that the initiated cracks propagated in the interface of zirconia post and IPS Empress 2 ceramic.

Conclusion: Based on the results of this study, inserting zirconia post (cosmopost) in IPS Empress 2 ceramic does not reinforce all-ceramic inlay retained resin bonded fixed partial dentures.

---

Background and Aim: Considering flexural strength of fiber-reinforced composites (FRC) and also the role of conservative cavities in protecting sound tissue of abutments, the aim of this study was to evaluate the fracture resistance of these bridges by handmade samples in vitro.

Materials and Methods: In this experimental in vitro study, 44 sound newly extracted teeth were used to make 22 fixed inlay bridges including 11 three unit anterior upper inlay bridges substituting clinical model of upper central and 11 three unit posterior lower inlay bridges substituting clinical model of lower first molar. Specimens were prepared with FRC and mounted with artificial PDL in acryl. Cases were exposed to final load by using Universal Testing Machine (Instron 1195) with the speed of 1 mm/min. Statistical analysis was performed by Kolmogorov- Smirnov, independent sample T and Kaplan-Meier tests with p<0.05 as the level of significance.

Results: Based on the statistical tests, the 95% confidence interval of mean was 450-562 N in anterior and  1473- 1761 N in posterior area. Fracture strength was high in the studied groups. Fractures in both groups occurred on composite facing, and the framework remained intact. The highest percentage of fracture in posterior teeth was in the middle of pontic towards the distal connector and in the anterior teeth in the lateral connector, between central pontic and lateral abutment. Using the independent sample T  test a significant statistical difference was observed between two groups (P<0.001). The fracture resistance of anterior samples was lower than the posterior ones.

Conclusion: Based on the results of this study regarding the high fracture resistance in both areas FRC inlay bridges could be recommended for upper anterior and lower posterior teeth in clinical dentistry certainly more studies are needed to ascertain this treatment option.

---

Background and Aim: The use of fiber reinforced posts in endodontically treated teeth has become increasingly common. But their retention in root canals must be considered seriously. The aim of this study was to evaluate the effect of light-cure and dual-cure bondings on regional bond strength of a fiber composite post.

Materials and Methods: In this experimental in vitro study, 20 endodontically treated teeth were randomly divided into two groups. In the first group, a dual-cure bonding (Scotchbond Multi-Purpose Plus, 3M ESPE/USA) [SBMP] was used and in the other group, a light-cure bonding (Single Bond, 3M ESPE/USA) [SB] was applied according to the manufacturer's instructions. A dual-cure resin cement (Rely X ARC, 3M ESPE/USA) was used to cement the post (Glassix, Harald Nordin SA,Switzerland). Coronal 8mm of cemented posts were sectioned in equal thirds using a 0.1mm diamond disc. Each slice was polished by a soft and wet abrasive paper in order to get a 2mm thickness. Loading was performed by a testing machine (Zwick/Germany) at a speed of 1mm/min until the post was dislodged. Data were analyzed using one-sample Kolmogorov-Smirnov, T and ANOVA tests with P<0.05 as the level of significance.

Results: There was a significant difference between the two adhesive systems in the middle third of the canal block with higher bond strength in SBMP group (p=0.02). In SB group the bond strength of the cervical region was higher than the middle and apical thirds (p<0.05). In SBMP group, there was no statistically difference between bond strength of the three regions (p=0.117).

Conclusion: Based on the results of this study, dual-cure bonding could be recommended for composite post cementation into root canals, because its bond strength was more uniform in different regions of root and greater in the middle and third regions.

---

Background and Aim: Various studies have shown that reliable bond at the root - post - core interfaces are critical for the clinical success of post - retained restorations. Severe stress concentration at post - cement interface increases post debonding from the root. To form a bonded unit that reduces the risk of fracture, it is important to optimize the adhesion. Therefore, some post surface treatments have been proposed. The purpose of this study was to investigate the influence of various surface treatments of tooth - colored posts on the bonding of resin cement.

Materials and Methods: In this interventional study, 144 tooth colored posts were used in 18 groups (8 samples in each group). The posts included quartz fiber (Matchpost), glass fiber (Glassix), and zirconia ceramic (Cosmopost) and the resin cement was Panavia F 2.0. The posts received the following surface treatments: 1- No surface treatment (control group), 2- Etching with HF and silane, 3- Sandblasting with Cojet sand, 4- Sandblasting with Cojet sand and application of silane, 5- Sandblasting with alumina particles, 6- Sandblasting with alumina particles and application of silane. Then, posts were cemented into acrylic molds with Panavia F 2.0 resin cement. The specimens were placed in water for 2 days and debonded in pull - out test. Statistical analysis was performed using ANOVA followed by Tamhane and Tukey HSD. Failure modes were observed under a stereomicroscope (10 ). P<0.05 was considered as the significant level.

Results: Surface treatments (sandblasting with Cojet and alumina particles ,with or without silane) resulted in improved bond strength of resin cement to glass fiber post (Glassix) and zirconia ceramic (Cosmopost) [p<0/05], but not to the quartz fiber post (Matchpost). In general, higher bond strengths resulted in a to higher percentage of cohesive failures within the cement.

Conclusion: Based on the results of this study, sandblasting with cojet and alumina particles increases bond strength of resin cement to glass fiber post (Glassix) and zirconia ceramic (Cosmopost).Generally, the bond strength of resin cement to the posts is affected by the post's composition and surface treatment.

---

Background and Aim: Nonmetallic tooth- colored posts adhere to canal walls by dentin bonding agents and resin cements. Better retention and proper distribution of stress result from enough and proper bonding. The purpose of this study was to evaluate bond strength of D.T. Light - post with two different resin cements (self-cure & dual-cure) and to investigate the effect of irrigating solutions applied in root canal on bond strength of the resin cements and D.T.Light- post to root canal wall.

Materials and Methods: In this experimental study 40 single root teeth (maxillary canine & central) were selected and stored in 0.1% thymol solution for one week and transferred to distilled water. The teeth were decoronated 2mm above CEJ. The canal space was mechanically enlarged using k-files (up to # 70). The teeth were randomly divided into two groups. The first group was irrigated with 2.6% NaOCl, and the second was irrigated with normal saline. After drying, the teeth were filled with gutta percha cones using lateral condensing method. After two weeks the post space was prepared and D.T.Light- post was inserted in each subgroup using self or dual-cure cements according to manufacturer's instructions. After thermocycling, the apical part was cut 1cm below CEJ. The remained length was divided into 9 equal sequential sections. Each section was submitted to shear push-out test in universal testing machine. Statistical analysis of the bond strength data was performed using ANOVA and post hoc tests with p<0.05 as the level of significance. All failed specimens were examined under stereomicroscope. Degrees of conversion of the cements were determined by FTIR.

Results: Significant difference in bond strength values were found among sites (P=0.001) and cements (P=0.03). With increasing in depth, bond strength decreased. The mean bond strength value in dual-cure resin cement was higher than self-cure cement. The irrigating solutions caused no significant difference in bond strength (P=0.46). DC% had significant difference in various depths.

Conclusion: According to the results of this investigation, bond strength of dual-cure cement is higher than self-cure one in D.T Light- post because of post's translucency. 2.6% sodium hypochlorite does not affect the bond strength.

---

Background and Aim: Fractured anterior teeth can be restored by adhesive bonding of the separated fragment to the remaining tooth structure. This invitro study evaluated the force required for fracture of rebonded fragments which were dried and rewetted for various time intervals prior to bonding.

Materials and Methods: One hundred and eight human mandibular incisors were selected and were divided into 9 groups and then were fractured. The fragments were stored in air at room temperature and ambient humidity. They were air dried for 30 minutes in group 1, 2 and 3,  6 h in group 4 and 5,  24 h in group 6 and 7, and 3 days in groups 8 and 9. The apical parts of the fractured teeth were stored in water.After storage in air, each fragment in group 1 was bonded to the remaining apical tooth structure with a bonding agent and flowable composite.In groups 2, 4, 6 and 8 after air drying the fragments were stored in water for 30min. The time of storage in water in groups 3, 5, 7, 9 was 24 hours. Then each fragment was bonded to the apical part structure. The mean force required for fracture was measured by a mechanical testing machine. One way ANOVA and Tuckey tests were used for analysis.

Results: There were statistically significant differences between different groups (p<0.001).The highest and lowest force required for fracture belonged to groups 3 and 8 respectively. The force required for fracture in group 1 was lower than group 2, 3, 5 and 7 and 9 and more than groups 4,6 and 8 with significant differences.While there were no significant differences among groups 3, 5, 7, 9 and 4, 6, 8 the force required for fracture in groups 2, 3, 5, 7 and 9 was more than 4, 6, 8 with significant differences.

Conclusion: This research revealed that the force required for fracture was affected by air storage of fragments prior to bonding. Also showed that with an increase in duration of drying the force required for fracture decreased and after a period of time it becomes steady. This study showed that in order to increase the fracture strength after air drying the fragment should be immersed in water for at least 24 hours prior to bonding.

---

Background and Aim: As composite-dentin bond strength is affected by cavity preparation and the bond strength of composite resin to new and used bur prepared dentin has not yet been evaluated, this study evaluated the effects of cutting dentin with different cutting efficacy (new and used) of burs on composite-dentin shear bond strength using self-etching primer bonding system and total etching bonding system.

Materials and Methods: Sixty caries free human 3rd molar were sectioned in occlosal surface to expose dentin, then polished with silicon carbide paper and randomly divided into four groups. Each group was prepared in a depth of 0.5mm of dentin, using new diamond bur, or used diamond bur. To change into a used bur, each new rough diamond bur had to work on bovine enamel for 30 minutes, under a load of 150g. Then, each group was bonded, using a total etch adhesive (single Bond) or a self etch adhesive (clearfil SE Bond) So there were 4 groups : 1-SE Bond, New bur 2-SE Bond , used bur 3-Single Bond , New bur 4-Single Bond, used bur. Similar composite capsules(Filtek Z250) were bonded to dentin surface and cured. specimens were stored in physiologic saline for 48h at 37⁰ c , then put under shearing load to define composite - dentin shear bond strength. Results were interpreted via statistical analysis (T-test & two - way variance).

Results: Shear bond strength of each group was as follows: 1-(27.3Mpa), 2-(33.5Mpa), 3-(16.9Mpa) 4-(19.3Mpa). Statistical analysis proved that shear bond strength of used diamond bur prepared groups (2,4) was more than new diamond bur prepared ones (1,3). This statistical difference, specially, was seen between SE Bond groups (1,2) but not between single Bond groups (3,4). Also, shear bond strength of (SE Bond) bonded groups (1,2) were more significantly than (single Bond) bonded ones (3,4).

Conclusion: This study show that Bur cutting efficiency influences composite - dentin shear bond strength especially when the adhesive is SE Bond (used bur> new bur) Also type of adhesive affects on composite - dentin shear bond strength. (SE Bond > Single Bond).

---

Background and Aim: Debonding is the most common failure type of fiber posts. This in vitro study aimed to evaluate the bond strength of 3 different fiber posts cemented with a resin luting agent in three regions of prepared post spaces after being subjected to termocycling.

Materials and Methods Thirty six mandibular first premolars were sectioned at the cemento-enamel junction and were treated endodontically. After one week the post spaces were prepared and roots were divided into 3 groups of 12 specimens according to the post types (D.T.Composipost, D.T.White, D.T.Light). Sealbond Cement Dual II was used in all groups. One day after cementation, specimens were subjected to 3500 thermal cycles (5^oC/55^oC). Each root was then embedded in acrylic resin and sectioned perpendicular to long axis. Three 1-mm tick segments from apical, middle and cervical thirds were prepared. Push out test was performed. Data were analyzed with 2-way ANOVA (P<0.05). All root segments and dislodged posts were observed with stereomicroscope to figure out their failure modes.

Results: The post type had no significant effect on bond strength (p=0.08). However bond strength at the coronl segment was higher than the other segments (p=0.005). Mixed mode was the mostly occurred failure mode with D.T.Composipost and D.T.Light but with D.T.White, the mostly occurred failure mode was adhesive between the post and cement.

Conclusion: Different fiber posts have relatively similar bond strength to root dentin, bond strength at the coronl segment was higher than the other segments.